The current method describes the simultaneous equation spectrophotometric method for the estimation of diloxanide furoate and ornidazole from their combined tablet dosage form by using Methanol as a solvent. The two wavelength 259 nm for diloxanide furoate and 312 nm for ornidazole were used for the estimation of diloxanide furoate and ornidazole. The method follows beer’s linearity in the range of 2-10 µg/ml for diloxanide furoate and 2-16 µg/ml for ornidazole. The % recovery was found to be 99.64–100.33 % for diloxanide furoate and 99 - 99.91% for ornidazole. The proposed method has been validated as per ICH guidelines and successfully applied to the estimation of diloxanide furoate and ornidazole from their combined Tablet dosage form.
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